By Uncle Fester
In regards to the Author
I am commonly thought of to be the founding father of the sphere of clandestine chemistry in its smooth shape. within the greater than 25 years that i've been writing books, i've got reworked this box from one packed with secrets and techniques and hocus pocus right into a actual technological know-how. i've got additionally been the teacher of the champions of this box during the many books i've got written through the years. you could learn even more approximately me through vacationing my site.
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Extra resources for Advanced Techniques Of Clandestine Psychedelic & Amphetamine Manufacture
Have clean hands to avoid smearing grease on the screen. Next thread a copper wire through the screen near its top edge, and twist it down tightly to assure good electrical contact. Then immerse the copper or brass screen in 5% hydrochloric acid solution for about 30 seconds or so. This removes oxides from the surface of the copper or brass, and leaves the surface active and ready to accept an adherent electroplate. Rinse the screen in clean water. You will note that the screen is now more reddish colored.
A screen about 3 em high, and 20 em long would nicely line the lower inside wall of the beaker. 8 ml of acetic acid, and 3 ml water in 100 ml of methanol is made up, and the majority of it is added to the beaker. Enough is poured into the rubber to equalize the liquid depth inside the beaker and the rubber. One must get this solution into the beaker before the screen dries out, because dried Raney nickel will start fires. The screen must be completely submerged by the solution. Next, connect the screen to the negative pole of a DC transformer.
First some toluene-water azeotrope distills at 85° C. It has a milky appearance. Then pure toluene distills at 110° C. When most of the toluene has distilled out, heating is Chapter Six A New Low Profile Phenylacetone Synthesis 53 stopped, and a vacuum is applied from an aspirator, cautiously at first to keep the distilling pot from boiling over. Then full vacuum is applied, and heating begun again. A good aspirator will distill phenylacetone at about 120-130 0 C. If the water isn't very cold where you live, the temperature will be correspondingly higher.