Chemorheology of Thermosetting Polymers by Clayton A. May (Eds.)

By Clayton A. May (Eds.)

content material: approach automation : a rheological and chemical assessment of thermoset curing / C.A. may perhaps, M.R. Dusi, J.S. Fritzen, D.K. Hadad, M.G. Maximovich, K.G. Thrasher, and A. Wereta, Jr. --
remedy kinetics and mechanical homes of a resin matrix : results of impurities and stoichiometry / Gary L. Hagnauer, Peter J. Pearce, Bernard R. Laliberte, and Margaret E. Roylance --
Kinetics of acetylene-terminated resin remedy and its results on dynamic mechanical homes / I.J. Goldfarb, C.Y-C. Lee, and C.C. Kuo --
Acetylene-terminated resin treatments : air and nitrogen results / C.Y-C. Lee, C.C. Kuo, and I.J. Goldfarb --
Mechanism and kinetics of the curing technique in a resin approach / J. Moacanin, M. Cizmecioglu, S.D. Hong, and A. Gupta --
Moisture-temperature results at the dynamic mechanical houses of epoxy polymers / Wayne J. Mikols and James C. Seferis --
Cross-linking response of an epoxy resin with phthalic anhydride / Elbert W. Crandall and Winston Mih --
Chemiluminescence of thermosetting resins / Clarence J. Wolf, Dale L. Fanter, and Michael A. Grayson --
Poly(n-butyl methacrylate) and poly(butyl methacrylate-co-acrylic acid) motion pictures : dried from recommendations of hydrogen bonding power / Michael S. Chuu, Carl J. Knauss, Richard J. Ruch, and Raymond R. Myers --
medication of intaglio printing inks / D.L. Hunston, J.L. Rushford, W.R. Newitt, and B.A. Vandreuil --
Curing habit of segmented polyurethane adhesives / D. Mark Hoffman --
Rheological treatment transformation diagrams for comparing polymer healing dynamics / Richard J. Hinrichs --
Curing kinetics of unsaturated polyester and vinyl ester resins / Chang Dae Han and Kwok-Wai Lem --
Dynamic mechanical and dielectric homes of an epoxy resin in the course of therapy / W.X. Zukas, W.J. Macknight, and N.S. Schneider --
Reactive structures : finite point research / Craig Douglas and David Roylance --
Kinetic version of remedy reactions : aids to estate and processing predictions / H.S.-Y. Hsich, R.M. Zurn, and R.J. Ambrose --
Thermosetting coatings : analytical and predictive strength by way of chemorheology / Richard R. Eley --
Predictive versions as aids to thermoset resin processing / M.R. Dusi, C.A. might, and J.C. Seferis.

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POLYMERS HAGNAUER ET AL. Impurities and Stoichiometry of Resin Matrix •-ν ι •cΗ ε νΟ νΟ ο 00 •Η Ο ο CvJε ο ο CM οοι Ο rH CM CO C ο •Η CM ο • β •p CO rH Φ c φ CO Q Ω s -Ρ < Σ • • CvJ οο • ο ο CO ON CO CvJ • • • 00 c ε C νΟ 00 ο ο ίί oc • 00 CvJ eu ο • νΟ • 00 • ο CvJ CO ινΟ m CvJ σ\ CO *^ • • ν— ST Ο Ε­ Ο ^· Φ •Ρ ί­ ο CM to Jφ •Ρ χ—\ νΟ τ— ΟΟ I χα. Ο CO Η mi • Μ Μ Μ CO • • • CO σ Φ σ • ο Φ %* CvJ c*— CO C0 CO < < *^ C0 Φ rH ο ο α< ε CO C O ο. ; ACS Symposium Series; American Chemical Society: Washington, DC, 1982.

5093) and Glyamine G-120 (Lot No. 1003) were obtained from Ciba Geigy Corp. , r e s p e c t i v e l y , and were stored i n c l o s e d c o n t a i n e r s a t -13 C. The samples designated TGMDA and ••Residue" were i s o l a t e d from the G-120 r e s i n u s i n g p r e p a r a t i v e l i q u i d chromatography OK Sample TGMDA i s e s s e n t i a l l y pure monomer; whereas the Residue c o n s i s t s p r i m a r i l y o f higher molecular weight oligomers and r e l a t i v e l y p o l a r r e s i n components.

P o i n t s No. 2,3,4,6 i n t h e p r e v i o u s paper (7) which a r e a t low enough temperatures t o be t h e instantaneous Τ f o r t h e r e a c t i o n time given i n t h e l a s t column o f Table I . By comparison w i t h F i g u r e 1, one o b t a i n s t h e value o f <* f o r each time. P o i n t s No. 5 and 8 r e p r e s e n t t h e time to reach a l o s s modulus maximum a t 130 and 180° r e s p e c t i v e l y . So once again α can be obtained from t h e time from F i g u r e 1. P o i n t s No.

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