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The chemically modified ACs, along with a commercial AC (S208c), were saturated with ortho- (OCP) and meta-chlorophenol (MCP) to investigate the potential for thermally regenerating the spent ACs. The thermal regeneration process was monitored by thermal analysis (TGA/DSC), gas chromatography and mass spectrometry (GC/MS). Thermal desorption profiles showed that in most cases weight losses occur in two steps (weak physisorption at ~220°C and strong chemisorption at ~620°C). Intermediate steps at ~400°C appeared in samples whose chemical treatments successfully weakened the interactions between strongly chemisorbed CP molecules and AC surfaces.
GAVEL results can be friendly used for point and regional ground water vulnerability assessment, as well for the mapping of the data. The proposed GAVEL application was successful tested for two test sites (Moldova and Germany). The Total Dissolved Solids is the most convenient parameter both from methodological and analytical conditions. Data of this scientific investigation permit to place the GAVEL method among the internationally existing approaches for ground water vulnerability estimation related to surface pollutants.
The regularities and effectivity of 43 ECOLOGICAL CHEMISTRY, 2005, Chisinau, Republic of Moldova both systems used have been compared. It was determined the chemical oxigen demand (COD) by oxidation with potassium dicromate in sulfuric acid and heating for two hours. COD varies from 4 to 94% depending on the system used. The main steps of the primary purification of polluted waters from dyes are proposed. The catalymetric method for the determination of the microquantities of manganese in natural waters on the basis of catalytic system Mn(II)-HCO3- -H2O2S (S- acid anthraquinone dyes has been elaborated.